Author(s): R. Swetha Sri, S. Jaya Sri, M. Sumakanth

Email(s): swetha.remidicharla@gmail.com

DOI: 10.52711/2349-2988.2024.00002   

Address: R. Swetha Sri1*, S. Jaya Sri2, M. Sumakanth3
1Assistant Professor, Department of Pharmaceutical Analysis, RBVRR Women’s College of Pharmacy, Barkathpura, Hyderabad - 500027, Telangana, India
2Research Student, RBVRR Women’s College of Pharmacy, Barkathpura, Hyderabad - 500027, Telangana, India
2Head of the Institution, RBVRR Women’s College of Pharmacy, Barkathpura, Hyderabad - 500027, Telangana, India
*Corresponding Author

Published In:   Volume - 16,      Issue - 1,     Year - 2024


ABSTRACT:
A facile and cost effective conductometric method for quantitative estimation of vanillin content in various locally available brands of vanilla custard powders was performed. Background of the study was conducted taking the base of varied consumption of flavored foods. Vanillin being the choice of flavored desserts in the local region of Telangana, few brands of custard powder were analyzed conductometrically. The milk proteins were removed by precipitation using Saturated copper sulphate and the vanillin content of the various vanilla flavoured custard powder was extracted by liquid-liquid extraction using methanol as solvent.Then the extracted analyte was titrated aganist 0.00105 M NaOH (Standardized).The observed conductance readings on Y-axis and volume of NaOH added on X-axis was taken and plotted a graph and end point determined graphically at 3.5mL,4mL and 3.5mL for product-1, product-2 and product-3.The amount of vanillin content in various locally available brands of vanilla flavoured custard powders was determined. And all the data obtained in this study was within the limits according to FDA. This method is well suited for routine lab analysis and easy to perform when compared to spectroscopic methods.


Cite this article:
R. Swetha Sri, S. Jaya Sri, M. Sumakanth. Quantitative Estimation of Vanillin content in various brands of Vanilla Flavored Custard Powder by Conductometry . Research Journal of Science and Technology. 2024; 16(1):6-0. doi: 10.52711/2349-2988.2024.00002

Cite(Electronic):
R. Swetha Sri, S. Jaya Sri, M. Sumakanth. Quantitative Estimation of Vanillin content in various brands of Vanilla Flavored Custard Powder by Conductometry . Research Journal of Science and Technology. 2024; 16(1):6-0. doi: 10.52711/2349-2988.2024.00002   Available on: https://rjstonline.com/AbstractView.aspx?PID=2024-16-1-2


REFERENCES:
1.    Ohashi M., Omae H., Hashinda M., Sowa Y. Determination of vanillin and related flavour compounds in cocoa drink by capillary electrophoresis. J Chromatogr A. 2007; 1138(1-2).
2.    Katherine K., Solmaz K. Quantitative Determination of Vanillin in Coated Paper Using Gas Chromatography, IOP Conference Series Material Science and Engineering. 2020; 742(1).
3.    Zhiyuan W., Guangfeng Z., Xiaoqun W., Bo Ding. Determination of Vanillin and Ethyl vanillin in MIlk Powder by Headspace Solid-Phase Microextraction Coupled With Gas Chromatography-Mass Spectroscopy. Food Anal Methods. 2016; 9(12).
4.    Qu B, Jiang J, Mao X, et al. Simultaneous determination of vanillin, ethyl vanillin and methyl vanillin in Chinese infant food and other dairy products by LC-MS/MS, Food Addit contend Part A. Chem Anal Control Expo Risk Assess. 2021; 38(7): 1096-1104. doi:10.1080/19440049.2021.1902573
5.    Banjoko O.O., Gbadamosi M.R., Moyib O.K., Ogunneye A.L., Oladapo F.O. Poast-column derivatization and quantitative determination of vanillin in Ice cream and Custard powder by High Performance Liquid Chromatography (HPLC). Niger J Chem Res. 2018; 23(1): 1-9.
6.    Krishna Veni. N., Meyyanathan. S N., Akilesh Reddy. A., Sagar. K. Analysis of vanillin in food products by High performance thin layer chromatography. Environmental Science. 2013.
7.    Rind. F.M.A., Alamani. F., Rehman. U. Spectrophotometric Analysis of Vanillin from Natural and Synthetic Sources. Asian J Chem. 2009; 21(4): 2849-2856.
8.    Upendra K Sharma, Arun k Sinha. A Comprehensive Review on Vanilla Flavor: Extraction, Isolation and Quantification of Vanillin and Others Constituents. Intl Sci. Food and Nutrition. 2007; 59(4):299-32.
9.    D. M. Freeland. The extraction and determination of vanillin in chocolate and cocoa butter. Analyst.1932:670.
10.    Ohashi M, Omae H, Sowa Y. Determination of vanillin and related flavor compounds in cocoa drink by capillary electrophoresis. J Chromatogr A. 2007; 1138(1-2): 262-7.
11.    Maria Jesus Lerma-Garcia., Ana Fuentes. Control of undeclared flavoring of cocoa powders by the determination of vanillin and ethyl vanillin by HPLC. Food Control. 2016: 171-176.
12.    Li Hayin, Mou Enming., Tang Danyu. Determination of vanillin in chocolate by rapid column high performance liquid chromatography. Journal of Anhui Agricultural Sciences. 2011; 37: 9841-9842.
13.    Jin Zhao, Haixiong Xia, Zhixu He. A Colorimetric assay for vanillin detection by determination of  O- toludine condensates. 2018;13(4).
14.    Yavuz Yardim, Mehmet Gulcan, Zuhre Senturk. Determination of vanillin in commercial food products by absorptive stripping voltammetry us in borond oped diamond electrode. Food chemistry. 2013; 141(3):1821-7.
15.    Preethi G. Pai, Pradeepti, Umma Habeeba, Sheetal Ullal. Evaluation of diuretic activity of Vanillin in healthy Wistar Albino rats. Research J. Pharm. and Tech. 2012; 5(9): 1246-1249.
16.    Khudhayer J. Kadem, Murad G. Munahi. Synthesis, Characterization and Biological Evaluation of some Novel 1,3 Oxazepine derivatives from Vanillin Schiff’s Bases. Research J. Pharm. and Tech. 2018; 11(9): 4047-4050.
17.    P. Saifulla Khan, P. Raveendra Reddy, V. Krishna Reddy. Utility of Schiff’s base Formation Reactions for the Spectrophotometric Determination of Pemetrexed Disodium in bulk and in its Pharmaceutical Formulations. Asian J. Research Chem. 2014; 7(3): 323-326.
18.    Rakesh Jasrai, Karan Singh Bhau, Nayana Bhrambhatt. Corrosion Inhibition of Zinc in Hydrochloric Acid by Vanillin, Phenyl Thiourea and N-Allyl Thiourea. Asian J. Research Chem. 2014; 7(12): 1062-1064
19.    S. N. Battin, A. H. Manikshete, S. K. Sarasamkar, M. R. Asabe, D. J. Sathe. Synthesis, Spectral, Antibacterial, Antifungal and Anticancer activity Studies of Schiff bases Derived from O-Vanillin and Aminoquinolines. Asian J. Research Chem. 2017; 10(5): 660-668.
20.    Pranali Gund, Shrikrishna Baokar, Santosh Undare. Difference spectrophotometric method development for the estimation of Acyclovir. Research J. Pharma. Dosage Forms and Tech. 2013; 5(2): 88-90
21.    Pravin Cholke, S.Z. Chemate, R.S. Joshi, M.A. Raskar, R.L. Sawant. Development and Validation of Spectrophotometric Method for Efavirenz in Pure and in Film Coated Tablet Dosage Form. Research J. Pharm. and Tech. 2011; 4(12): 1816-1818.
22.    Satish Middi, Shobha Manjunath. Development and Validation of Spectrophotometric Methods for Quantitative Estimation of Pramipexole Dihydrochloride in bulk and Pharmaceutical Dosage Form. Research J. Pharm. and Tech. 2012; 5(6): 764-767.
23.    Sudha. R, Nithya. G. Conductometric Studies On 3, 5-Dinitro Salicylic Acid in Ethanol Water Mixed Solvent Media. Research Journal of Pharmacy and Technology. 2021; 14(4):1989-2.
24.    M. Mukkanti Eswarudu, A. Lakshmana Rao, K. Vijay. Bioanalytical RP-HPLC Method for Simultaneous Quantification of Rivaroxaban and Ticagrelor in Spiked Human Plasma: Validation and Stability. Research Journal of Pharmacy and Technology. 2023; 16(6): 2741-6.


Recomonded Articles:

Author(s): M. Sandhya Rani, C. Rohini, B. Sai keerthi, C. Mamata.

DOI: 10.5958/2349-2988.2019.00028.7         Access: Open Access Read More

Research Journal of Science and Technology (RJST) is an international, peer-reviewed journal, devoted to science and technology...... Read more >>>

RNI: Not Available                     
DOI: 10.5958/2349-2988 


Recent Articles




Tags